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Reflux. 11) Take TLC at 45 min (showed most nitroethane had reacted, but a faint spot left), 1 h (wrong eluent), and at 1 h 15 min, can conclusively see that the conversion is fully complete. So once reflux begins, 1 hour is enough. The reaction is over. Might have taken TLC to check whether truly all of the nitrostyrene had been reduced.
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