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Beforehand, 50 mg of the benzaldehyde was dissolved in 2 mL IPA and kept in a glass vial. This was the benzaldehyde standard (labelled as Be on the plates). Run TLC on the first plate 35 min after the addition of the 2-HEAA in hopes of seeing something unexpected. The reaction mixture I draw with a regular pipette and dilute one drop with 0.5 mL fresh IPA.
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