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The DCM pulls the Be spot too high, This eluent mixture was more polar than hexane and ethyl acetate one. 10) After 3h TLC shows that much 3,4,5-TMBA remains, so at 3 h 20 min add 30 mL more NM. 11) Made a few more TLC plates and finally after about 7 hours of the reaction running between 50 — 60 °C but mostly at 55 °C, with gentle magnetic stirring, TLC shows only the faintest or no 3,4,5-T MBA spot.