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There is significant colour change at this point, and the liquid is turning more and more yellow. Smoke or some sort of mist forms on the surface of the reaction mixture after addition of MEA, suck it away. 8) Take TLC after 1 h 45 min and it does seem to show two spots with some sort of product, a tail above the 3,4,5-T MBA, but there is clearly lots of unreacted BA left.